Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitrite → N-Nitrosodiphenylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitrite | HCID 946 | — |
| 반응물 | Diphenylamine | HCID 11487 | — |
| 생성물 | N-Nitrosodiphenylamine | HCID 6838 | — |
반응 단계
diphenylamine method, where diphenylamine as raw material is nitrosated using a nitrite in an organic solvent to produce N-nitrosodiphenylamine, which is rearranged to 4-nitrosodiphenylamine hydrochloride under the action of anhydrous hydrogen chloride, and then, 4-nitrosodiphenylamine hydrochloride is neutralized with a base to give 4-nitrosodiphenylamine which is finally reduced to 4-aminodiphenylamine by sodium sulfide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07084302B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-e70b01ed6e6a4bcc904277bc74d3110e |
| 출처 메모 | uspto-grants-2006_08 |