Diethyl Ether → HCID 178496926, 화합물

HRID 726643노트

반응식

HRID 726643 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:7]([NH2:11])=[CH:8][C:9]=1[Cl:10])[CH:5]=O.C[C:13](C)([C:17]([O-:19])=[O:18])[C:14]([O-:16])=O.[CH2:21](OCC)C>>[Cl:1][C:2]1[CH:3]=[C:4]2[C:7](=[CH:8][C:9]=1[Cl:10])[N:11]=[C:14]([OH:16])[C:13]([C:17]([O:19][CH3:21])=[O:18])=[CH:5]2

참가 물질

4

반응물 3

HCID 3283Diethyl EtherHCID 8180132-Amino-4,5-dichlorobenzaldehydeHCID 6946994Dimethylmalonat

생성물 1

HCID 178496926HCID 178496926, 화합물

실험 절차

3,4-Dichloro-6-aminobenzaldehyde (2.85 g, 15 mmol) was stirred with dimethylmalonate (10 ml) at 140° C. for 20 h. The mixture was diluted with ethyl ether (100 ml). The precipitate was collected, washed twice with ethyl ether and dried in vacuo to give 2.86 g of methyl 6,7-dichloro-2-hydroxyquinoline-3-carboxylate.

후처리

  1. customThe precipitate was collected
  2. washwashed twice with ethyl ether
  3. customdried in vacuo

출처 및 근거

ORD 기록
ord-23d4d49596454dcd92078d9946d5b5ab
출처 데이터셋
uspto-grants-1998_01
특허 번호
US05710139

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