Hexacyanocobalt → HCID 11125012, 화합물

HRID 726941노트

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HRID 726941 반응식
[C-:1]#[N:2].[C-]#N.[C-]#N.[C-]#N.[C-]#N.[C-]#N.[Co:13].[Cl-].[Zn+2:15].[Cl-]>O>[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[C-:1]#[N:2].[Co+3:13].[Co+3:13].[Zn+2:15].[Zn+2:15].[Zn+2:15]

참가 물질

4

반응물 2

HCID 407334HexacyanocobaltHCID 3007855Zincchloride

생성물 1

HCID 11125012HCID 11125012, 화합물

시약·촉매·용매 1

HCID 962Water용매3회

실험 절차

Potassium hexacyanocobaltate (4.0 g) is dissolved in deionized water (150 mL) in a beaker. Zinc chloride (10 g) is dissolved in deionized water (15 mL) in a second beaker. The aqueous solutions are quickly combined and magnetically stirred for 10 min. The precipitated solids are isolated by centrifugation. The solids are reslurried in deionized water (100 mL) for 10 min. with stirring, and are again recovered by centrifugation. The catalyst is dried in a vacuum oven at 50° C. and 30 in. (Hg) to constant weight. This catalyst is identified as Catalyst A, and has the powder X-ray diffraction pattern shown in FIG. 4.

후처리

  1. customThe precipitated solids are isolated by centrifugation
  2. stirringwith stirring
  3. customare again recovered by centrifugation
  4. customThe catalyst is dried in a vacuum oven at 50° C.

출처 및 근거

ORD 기록
ord-794d40a6200945d3ad81336bfb78cf19
출처 데이터셋
uspto-grants-1998_01
특허 번호
US05712216

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