Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)pyridine | HCID 70144893 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 70144331 | — |
반응 단계
A mixture of methyl iodide (0,5 ml, 7.5 mmol) and cis-3-(4-(3-hexenyloxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.9 g (46%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05712297 |
| 출처 데이터셋 | uspto-grants-1998_01 |
| ORD ID | ord-6734ddf93c8d4d62a799050c9c3e1fd8 |
| 출처 메모 | uspto-grants-1998_01 |