참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Iodine chloride | HCID 24640 | — |
| 반응물 | 2-Amino-5-bromobenzenesulphonic acid | HCID 15023615 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-Amino-5-bromo-3-iodobenzenesulphonic acid | HCID 18919385 | — |
반응 단계
To 45 g (176 mmol) of 2-amino-5-bromobenzenesulphonic acid are added 46 g (282 mmol) of iodine chloride, 400 ml of aqueous 1N hydrochloric acid solution and 400 ml of methanol. The mixture is heated at 90° C. for 18 hours and concentrated under reduced pressure, and the residue is crystallized from ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05712393 |
|---|
| 출처 데이터셋 | uspto-grants-1998_01 |
|---|
| ORD ID | ord-c7555d9d61194faeb8c71463882c07bf |
|---|
| 출처 메모 | uspto-grants-1998_01 |
|---|
