Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Ethyl 3-Fluoro-4-nitrobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 3-Fluoro-4-nitrobenzoic acid | HCID 230653 | — |
| 생성물 | Ethyl 3-Fluoro-4-nitrobenzoate | HCID 45036938 | — |
반응 단계
To the liquid mixture of 3-fluoro-4-nitrobenzoic acid 9.71 g and ethanol 35 mL, cone. sulfuric acid 1.6 mL was added, followed by 16 hours' heating under reflux. After distilling the solvent off, water and tert-butyl methyl ether were added to the residue. The organic layer was extracted, washed with water and dried over magnesium sulfate. Distilling the solvent off, 7.40 g of the title compound was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08829000B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-2186fce3620a40909637c4fd0559f38d |
| 출처 메모 | uspto-grants-2014_09 |