Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 3-Amino-2-phenylpropan-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Phenibut | HCID 14113 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | 3-Amino-2-phenylpropan-1-ol | HCID 11286566 | — |
반응 단계
For the preparation of the alcohols VI used in Examples (3a) and (3b). 10 g of 3-amino-2-phenylpropanecarboxylic acid in 150 ml of monoglyme were stirred with 3 g of LiAlH4 for 20 hrs. Then, 12 ml of water and 3 ml of 10% sodium hydroxide solution were slowly added thereto. The mixture was filtered and the filtrate was again evaporated with toluene. There was obtained 8.4 g of β-(aminomethyl)-phenethyl alcohol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05045567 |
| 출처 데이터셋 | uspto-grants-1991_09 |
| ORD ID | ord-94cfd474d910450e9c00447414ac647c |
| 출처 메모 | uspto-grants-1991_09 |