N,N-Dimethyltetradecylamine → Tetradecyldimethyl 2-acetyloxyethylammonium bromide
반응식
[C:1]([O:4][CH2:5][CH2:6][Br:7])(=[O:3])[CH3:2].[CH2:8]([N:22]([CH3:24])[CH3:23])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>CC(CC)=O>[Br-:7].[CH2:8]([N+:22]([CH3:24])([CH3:23])[CH2:6][CH2:5][O:4][C:1](=[O:3])[CH3:2])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]참가 물질
4
반응 조건
- 온도
- 90 °C
실험 절차
In a reaction vessel was placed 42.8 grams of 2-bromoethyl acetate, 58.9 grams of tetradecyldimethylamine and 107.6 grams of methylethyl ketone (MEK) solvent. The mixtures was refluxed (ca. 90° C.) under nitrogen with stirring for 7 hours. The reaction mixture was cooled and the solvent decanted leaving as the product tetradecyldimethyl 2-acetyloxyethylammonium bromide.