N,N-Dimethyltetradecylamine → Tetradecyldimethyl 2-acetyloxyethylammonium bromide

HRID 728383

반응식

HRID 728383 반응식
[C:1]([O:4][CH2:5][CH2:6][Br:7])(=[O:3])[CH3:2].[CH2:8]([N:22]([CH3:24])[CH3:23])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>CC(CC)=O>[Br-:7].[CH2:8]([N+:22]([CH3:24])([CH3:23])[CH2:6][CH2:5][O:4][C:1](=[O:3])[CH3:2])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

참가 물질

4

반응물 2

HCID 8211N,N-DimethyltetradecylamineHCID 135641-Acetoxy-2-bromoethane

생성물 1

HCID 14625468Tetradecyldimethyl 2-acetyloxyethylammonium bromide

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

반응 조건

온도
90 °C

실험 절차

In a reaction vessel was placed 42.8 grams of 2-bromoethyl acetate, 58.9 grams of tetradecyldimethylamine and 107.6 grams of methylethyl ketone (MEK) solvent. The mixtures was refluxed (ca. 90° C.) under nitrogen with stirring for 7 hours. The reaction mixture was cooled and the solvent decanted leaving as the product tetradecyldimethyl 2-acetyloxyethylammonium bromide.

후처리

  1. customIn a reaction vessel was placed
  2. temperatureThe reaction mixture was cooled
  3. customthe solvent decanted

출처 및 근거

ORD 기록
ord-ecf0276c9b984c51ba50ff4b67327c1f
출처 데이터셋
uspto-grants-1991_09
특허 번호
US05047577

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