Phthalimide → 3-hexadecylthio-2-(5-methyl-2H-tetrazol-2-yl)propylamine

HRID 728465노트

반응식

HRID 728465 반응식
[CH2:1]([S:17][CH2:18][CH:19]([N:22]1[N:26]=[N:25][C:24]([CH3:27])=[N:23]1)[CH2:20]O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].C(SCC(OC)C[NH2:48])CCCCCCCCCCCCCCC.C1(=O)NC(=O)C2=CC=CC=C12>>[CH2:1]([S:17][CH2:18][CH:19]([N:22]1[N:26]=[N:25][C:24]([CH3:27])=[N:23]1)[CH2:20][NH2:48])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

참가 물질

4

반응물 3

HCID 6809PhthalimideHCID 148349873-hexadecylthio-2-(5-methyl-2H-tetrazol-2-yl)propanolHCID 149922653-Hexadecylthio-2-methoxypropylamine

생성물 1

HCID 148350063-hexadecylthio-2-(5-methyl-2H-tetrazol-2-yl)propylamine

실험 절차

3-hexadecylthio-2-(5-methyl-2H-tetrazol-2-yl)propanol Vh1 is allowed to react and worked up by the same procedure as described in (3). The phthalimide compound: m.p. 82°-83° C. The summary of the experimental condition and the physical data of the product are listed in Tables 5 and 6.

후처리

  1. customto react

출처 및 근거

ORD 기록
ord-a3c7e40b1c2e45e49c5cfcddaa851122
출처 데이터셋
uspto-grants-1991_09
특허 번호
US05047540

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