Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3-Epoxypropyl 4'-methoxyphenyl ether → HCID 14739881, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3-Epoxypropyl 4'-methoxyphenyl ether | HCID 16646 | — |
| 반응물 | N-(2-Aminoethyl)-4-(1H-imidazol-1-yl)benzamide | HCID 14664358 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 14739881 | HCID 14739881 | — |
반응 단계
To a solution of 2.39 g (13.2 mmol) 1,2-epoxy-3-(4-methoxyphenoxy)propane in 25 mL methanol is added 3.05 g (13.2 g) N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide. The reaction mixture is stirred under a nitrogen atmosphere for 24 h. After this time, the precipitate is collected and recrystallized from ethanol to provide the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05051423 |
| 출처 데이터셋 | uspto-grants-1991_09 |
| ORD ID | ord-38e8628e4cb44652858f6f795a33044a |
| 출처 메모 | uspto-grants-1991_09 |