HCID 14998766, 화합물 → HCID 14998775, 화합물

HRID 728955노트

반응식

HRID 728955 반응식
[Br:1][C:2]1[CH:3]=[C:4]([N:10]2[CH2:15][CH2:14][N:13]([CH2:16][C:17]3[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[C:19]([O:25][CH3:26])[CH:18]=3)[CH:12]([C:27]([NH2:29])=O)[CH2:11]2)[CH:5]=[C:6]([O:8][CH3:9])[CH:7]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[Br:1][C:2]1[CH:3]=[C:4]([N:10]2[CH2:15][CH2:14][N:13]([CH2:16][C:17]3[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[C:19]([O:25][CH3:26])[CH:18]=3)[CH:12]([CH2:27][NH2:29])[CH2:11]2)[CH:5]=[C:6]([O:8][CH3:9])[CH:7]=1

참가 물질

3

반응물 2

HCID 14998766HCID 14998766, 화합물HCID 21226445Aluminium lithium hydride

생성물 1

HCID 14998775HCID 14998775, 화합물

실험 절차

In a manner similar to Preparation 2, react 4-(3-bromo-5-methoxyphenyl)-1-[(3,4-dimethoxyphenyl)methyl]-2-piperazinecarboxamide with lithium aluminum hydride to obtain the title compound.

후처리

  1. customIn a manner similar to Preparation 2

출처 및 근거

ORD 기록
ord-b8ee305417d34135b25162a31d5cecaf
출처 데이터셋
uspto-grants-1991_09
특허 번호
US05051422

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