Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibutylstannane → Bis(2-acetoxyethyl)dibutyltin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibutylstannane | HCID 6513 | — |
| 반응물 | Vinyl Acetate | HCID 7904 | — |
| 용매 | Cyclohexane | HCID 8078 | — |
| 생성물 | Bis(2-acetoxyethyl)dibutyltin | HCID 14512231 | — |
반응 단계
2.349 g (0.01 mole) of dibutyltin dihydride, 1.722 g (0.02 mole) of distilled vinyl acetate, and 2 g of anhydrous cyclohexane were placed in aPyrex® bowl thermostated at 25° C. The solution was exposed to ultraviolet radiation for 3 hours. The cyclohexane was then eliminated under vacuum at ambient temperature. The expected product was obtained pure in quantitative yield
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05051521 |
| 출처 데이터셋 | uspto-grants-1991_09 |
| ORD ID | ord-d9cd12070b32479cb60c77f684ed435e |
| 출처 메모 | uspto-grants-1991_09 |