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Vinyl Acetate → HCID 14512238, 화합물

HRID 729103
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HRID 729103 반응식
[C:1]1([SnH2:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:14]([O:17][CH:18]=[CH2:19])(=[O:16])[CH3:15]>C1CCCCC1>[C:14]([O:17][CH2:18][CH2:19][Sn:7]([CH2:19][CH2:18][O:17][C:14](=[O:16])[CH3:15])([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)(=[O:16])[CH3:15]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 7904Vinyl AcetateHCID 494678Diphenyltin dihydride

생성물 1

HCID 14512238HCID 14512238, 화합물

시약·촉매·용매 1

HCID 8078Cyclohexane용매

실험 절차

Stoichiometric amounts of diphenyltin dihydride and vinyl acetate were placed in a Pyrex® tube containing anhydrous cyclohexane. The reactionmixture was exposed to ultraviolet radiation for 1 hour at 30° C. The solvent was then eliminated at ambient temperature under vacuum. The product was obtained quantitatively and had the following formula:

후처리

  1. customwas then eliminated at ambient temperature under vacuum
  2. customThe product was obtained quantitatively

출처 및 근거

ORD 기록
ord-85e09626d20d43c48d0c9cc009d50428
출처 데이터셋
uspto-grants-1991_09
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05051521

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