Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4-Diaminotoluene → HCID 178428252, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4-Diaminotoluene | HCID 7261 | — |
| 반응물 | Nitrosoantipyrine | HCID 13443 | — |
| 반응물 | Sodium Perchlorate | HCID 522606 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178428252 | HCID 178428252 | — |
반응 단계
50 mmol of 1,5-dimethyl-4-nitroso-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in a solution of 850 ml of acetic acid and 1250 ml of water. This solution was admixed with 50 mmol of 4-methylbenzene-1,3-diamine and stirring was continued for 2 h 30 min. Sodium perchlorate was added to saturation, and the mixture was left to stand for 30 minutes at zero degrees.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07582123B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-337954db342c466cbcef6fe9888bb754 |
| 출처 메모 | uspto-grants-2009_09 |