Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
P-Anisidine → 4-[(4-Methoxyphenyl)amino]-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | P-Anisidine | HCID 7732 | — |
| 반응물 | 4-Chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 68662017 | — |
| 생성물 | 4-[(4-Methoxyphenyl)amino]-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 11695874 | — |
반응 단계
The title compound was prepared from 4-chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 4-methoxyaniline in a similar manner as described for e.g. Examples 9 and 13. 1H NMR (400 MHz, CD3CN): δ 7.67 (bs, 1H), 7.27-7.22 (m, 1H), 7.18-7.10 (m, 4H), 6.78-6.73 (m, 2H), 6.57-6.52 (m, 2H), 3.65 (s, 3H), 3.20 (s, 3H); Mass Spectrum: M+H+ 345.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07582629B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-281e18fb8f1c43d7bd4083f72d89ed51 |
| 출처 메모 | uspto-grants-2009_09 |