Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(5-Amino-1-benzofuran-2-yl)ethanone → HCID 11703944, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(5-Amino-1-benzofuran-2-yl)ethanone | HCID 3783367 | — |
| 반응물 | 4-Chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 68662017 | — |
| 생성물 | HCID 11703944 | HCID 11703944 | — |
반응 단계
The title compound was prepared from 4-chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 1-(5-amino-1-benzofuran-2-yl)ethanone in a similar manner as described for e.g. Examples 9 and 13. 1H NMR (400 MHz, CD3CN): δ 7.89 (bs, 1H), 7.38-7.37 (m, 1H), 7.25 (d, 1H), 7.16-7.10 (m, 4H), 7.09-7.03 (m, 3H), 3.22 (s, 3H), 2.50 (s, 3H); Mass Spectrum: M+H+ 397.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07582629B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-d648d65938054e8298ce91262b6cfa66 |
| 출처 메모 | uspto-grants-2009_09 |