4,6-Dichloro-2-(methylthio)pyrimidine → HCID 66991899, 화합물

HRID 733031노트

반응식

HRID 733031 반응식
Cl[C:2]1[CH:7]=[C:6](Cl)[N:5]=[C:4]([S:9][CH3:10])[N:3]=1.[CH2:11]([NH:13][C:14]1[CH:15]=[C:16]([OH:20])[CH:17]=[CH:18][CH:19]=1)[CH3:12]>>[CH3:10][S:9][C:4]1[N:5]=[C:6]([N:13]([CH2:11][CH3:12])[C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([OH:20])[CH:15]=2)[CH:7]=[C:2]([N:13]([CH2:11][CH3:12])[C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([OH:20])[CH:15]=2)[N:3]=1

참가 물질

3

반응물 2

HCID 805314,6-Dichloro-2-(methylthio)pyrimidineHCID 5789913-Ethylaminophenol

생성물 1

HCID 66991899HCID 66991899, 화합물수율 43%

실험 절차

This compound was obtained (yield 43%) based on the method described in Production Example 2B using 4,6-dichloro-2-methylthio-pyrimidine instead of the 4,6-dichloro-2-ethylpyrimidine, and using 3-ethylaminophenol instead of the 3-aminophenol.

후처리

  1. customThis compound was obtained (yield 43%)

출처 및 근거

ORD 기록
ord-0f359a5f0cf748a7bf91b8c4cc4a1844
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07589105B2

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