Hexane → 1-Bromo-4-[(1S,2R)-2-vinylcyclopropyl]benzene

HRID 73305

반응식

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C@H:8]2[CH2:10][C@@H:9]2[CH:11]=O)=[CH:4][CH:3]=1.[CH3:13]CCCCC>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C@H:8]2[CH2:10][C@@H:9]2[CH:11]=[CH2:13])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 8058Hexane

HCID 57515374trans-2-(4-Bromophenyl)cyclopropane-1-carbaldehyde

생성물 1

HCID 684062521-Bromo-4-[(1S,2R)-2-vinylcyclopropyl]benzene

실험 절차

The product from Example 30A was subjected to the conditions outlined in in Example 26E, followed by chromatography (100% hexane) to provide the title compound.

출처 및 근거

ORD 기록: ord-8d713e5b8d1849198efd8c6191541e4e
출처 데이터셋: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08829041B2

연결된 노트

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