참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,2,3,3,3-Pentafluoropropanol | HCID 9872 | — |
| 반응물 | Trifluoromethanesulfonic anhydride | HCID 67749 | — |
| 생성물 | 2,2,3,3,3-Pentafluoropropyl trifluoromethanesulfonate | HCID 2776019 | 97% |
반응 단계
A mixture of trifluoromethanesulfonic anhydride (40 mL, 0.24 mol) and 2,2,3,3,3-pentafluoropropanol (25 mL, 0.24 mol) was heated under argon at 90° C. overnight. Then, the crude mixture was distilled at atmospheric pressure to give the desired product as a colourless oil (97% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07589125B2 |
|---|
| 출처 데이터셋 | uspto-grants-2009_09 |
|---|
| ORD ID | ord-5c7fcfdc30414347a5f208e1333ccbe4 |
|---|
| 출처 메모 | uspto-grants-2009_09 |
|---|
