Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl vinyl ether → 6-(1-Ethoxy ethoxy)-2-naphthaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl vinyl ether | HCID 8023 | — |
| 반응물 | 6-Hydroxy-2-naphthaldehyde | HCID 2764110 | — |
| 반응물 | 6-Ethenylnaphthalen-2-ol | HCID 23135758 | — |
| 생성물 | 6-(1-Ethoxy ethoxy)-2-naphthaldehyde | HCID 23135759 | — |
반응 단계
The synthesis of 6-hydroxy-2-vinylnaphthalene (HVN) was carried out by three step reactions starting from 6-hydroxy-2-naphthaldehyde. In the first step, 6-hydroxy-2-naphthaldeyde (HNAL) was protected with ethyl vinyl ether to give 6-(1-ethoxy ethoxy)-2-naphthaldehyde (EENAL). This was followed by the Wittig reaction of EENAL to yield 6-(1-ethoxy ethoxy)-2-vinylnaphthalene. Finally, this was deprotected using pyridinium p-toluenesulfonate to yield 6-hydroxy-2-vinylnaphthalene (HVN).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07592125B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-44e49d36b8344373abadf1d19721e492 |
| 출처 메모 | uspto-grants-2009_09 |