Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl chloride → 4-Methoxybenzophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl chloride | HCID 7412 | — |
| 반응물 | Anisole | HCID 7519 | — |
| 생성물 | 4-Methoxybenzophenone | HCID 69146 | 47% |
반응 단계
370 mg of benzoylchloride were reacted with 12 ml anisole to give the benzoylated product 4-methoxybenzophenone in 47% yield. The catalyst used is a HS—AlF3 metal fluoride on a Al2O3 support prepared according to the present invention, which is used in an amount of 300 mg. The reaction is carried out in a discontinuous batch process at 60° C. under reflux with stirring.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07592287B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-a14a8e7438594020a2313d82de28bc73 |
| 출처 메모 | uspto-grants-2009_09 |