Benzoyl chloride → 4-Methoxybenzophenone

HRID 734191

반응식

HRID 734191 반응식
[C:1](Cl)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:10]1([O:16][CH3:17])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[CH3:17][O:16][C:10]1[CH:15]=[CH:14][C:13]([C:1]([C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[O:8])=[CH:12][CH:11]=1

참가 물질

3

반응물 2

HCID 7412Benzoyl chlorideHCID 7519Anisole

생성물 1

HCID 691464-Methoxybenzophenone수율 47%

실험 절차

370 mg of benzoylchloride were reacted with 12 ml anisole to give the benzoylated product 4-methoxybenzophenone in 47% yield. The catalyst used is a HS—AlF3 metal fluoride on a Al2O3 support prepared according to the present invention, which is used in an amount of 300 mg. The reaction is carried out in a discontinuous batch process at 60° C. under reflux with stirring.

출처 및 근거

ORD 기록
ord-a14a8e7438594020a2313d82de28bc73
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07592287B2

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