BROMINE CHLORIDE (BrCl) → HCID 69058650, 화합물

HRID 734818

반응식

HRID 734818 반응식
[Br:1][C:2]1[C:3]([C:15]#[CH:16])=[N:4][CH:5]=[C:6]([C:8]2[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][CH:9]=2)[CH:7]=1.I[C:18]1[CH:27]=[CH:26][C:21]([O:22][CH2:23][CH2:24][OH:25])=[CH:20][CH:19]=1.BrCl>>[Br:1][C:2]1[C:3]([C:15]#[C:16][C:18]2[CH:27]=[CH:26][C:21]([O:22][CH2:23][CH2:24][OH:25])=[CH:20][CH:19]=2)=[N:4][CH:5]=[C:6]([C:8]2[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][CH:9]=2)[CH:7]=1

참가 물질

4

반응물 3

HCID 61697BROMINE CHLORIDE (BrCl)2회HCID 35132082-(4-Iodophenoxy)ethanolHCID 86077051HCID 86077051, 화합물

생성물 1

HCID 69058650HCID 69058650, 화합물

실험 절차

The product was prepared analogously to Example 7.1e starting from 3-bromo-5-(4-chlorophenyl)-2-ethynylpyridine and 2-(4-iodophenoxy)ethanol. Yield: 0.18 g (28% of theoretical); C21H15BrClNO2 (M=428.706); calc.: molpeak (M+H)+: 428/430/432 (BrCl); found: molpeak (M+H)+: 428/430/432 (BrCl).

후처리

  1. customThe product was prepared analogously to Example 7.1e

출처 및 근거

ORD 기록
ord-6f6408511ff741ada781877c68211bd1
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07592358B2

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