Methanesulfonyl chloride → HCID 86601888, 화합물

HRID 735024

반응식

HRID 735024 반응식
[I:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][OH:10])=[CH:4][CH:3]=1.[CH3:11][S:12](Cl)(=[O:14])=[O:13]>>[CH3:11][S:12]([O:10][CH2:9][CH2:8][C:5]1[CH:6]=[CH:7][C:2]([I:1])=[CH:3][CH:4]=1)(=[O:14])=[O:13]

참가 물질

3

반응물 2

HCID 31297Methanesulfonyl chlorideHCID 30407702-(4-Iodophenyl)ethan-1-ol

생성물 1

HCID 86601888HCID 86601888, 화합물

실험 절차

Prepared analogously to Example 1.2.b. from 2-(4-iodophenyl)ethanol and methanesulfonic acid chloride. Yield: 5.7 g (77.4% of theory); C9H11IO3S (M=326.15); calc.: molecular ion peak (M)+: 326; found: molecular ion peak (M)+: 326.

후처리

  1. customPrepared analogously to Example 1.2.b

출처 및 근거

ORD 기록
ord-c86c91840cf64a11936104102b145a56
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07592373B2

연결된 노트

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