Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Dimethylpiperidine → 1-[2-(2-Methoxy-4-nitrophenoxy)ethyl]-3,5-dimethylpiperidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Dimethylpiperidine | HCID 118259 | — |
| 반응물 | 1-(2-Bromoethoxy)2-methoxy-4-nitrobenzene | HCID 12937254 | — |
| 용매 | Dichloromethane methanol | HCID 21226129 | — |
| 생성물 | 1-[2-(2-Methoxy-4-nitrophenoxy)ethyl]-3,5-dimethylpiperidine | HCID 68819560 | — |
반응 단계
Prepared analogously to Example 1.1.c. from 1-(2-bromoethoxy)-2-methoxy-4-nitrobenzene and 3,5-dimethylpiperidine. Yield: 0.4 g (48.1% of theory); C16H24N2O4 (M=308.38); calc.: molecular ion peak (M+H)+: 309; found: molecular ion peak (M+H)+: 309; Rf value: 0.5 (silica gel, dichloromethane/methanol (9:1)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07592373B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-c7e9ff6246084a478ad9260b6a18f537 |
| 출처 메모 | uspto-grants-2009_09 |