HCID 22185398, 화합물 → HCID 22185405, 화합물

HRID 735137노트

반응식

HRID 735137 반응식
[CH3:1][O:2][C:3]1[CH:17]=[C:16]([N+:18]([O-])=O)[CH:15]=[CH:14][C:4]=1[O:5][CH2:6][CH2:7][N:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1>ClCCl.CO>[CH3:1][O:2][C:3]1[CH:17]=[C:16]([NH2:18])[CH:15]=[CH:14][C:4]=1[O:5][CH2:6][CH2:7][N:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1

참가 물질

3

반응물 1

HCID 22185398HCID 22185398, 화합물

생성물 1

HCID 22185405HCID 22185405, 화합물

시약·촉매·용매 1

HCID 21226129Dichloromethane methanol용매

실험 절차

Prepared analogously to Example 3.1.b. from 4-[2-(2-methoxy-4-nitrophenoxy)ethyl]morpholine. Yield: 0.23 g (85.8% of theory); C13H20N2O3 (M=252.31); calc.: molecular ion peak (M+H)+: 253; found: molecular ion peak (M+H)+: 253; Rf value: 0.5 (silica gel, dichloromethane/methanol (9:1)).

후처리

  1. customPrepared analogously to Example 3.1.b

출처 및 근거

ORD 기록
ord-94ebb71a274e4e3fbb6d2539dae244f4
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07592373B2

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