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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 735920생성일: 2026년 10월 25일

4-(Trifluoromethyl)benzylamine → N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[4-(trifluoromethyl)-benzyl]amine

https://huagongshe.com/reaction/735920

반응식

참여 물질

역할이름HCID투입량
반응물4-(Trifluoromethyl)benzylamineHCID 76804—
반응물4-(Dodecyloxy)-1-naphthaldehydeHCID 85841201—
생성물N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[4-(trifluoromethyl)-benzyl]amineHCID 6718691966%

반응 단계

The same procedure as employed in the preparation of Example 226 (step a) but using 4-(dodecyloxy)-1-naphthaldehyde and 4-(trifluoromethyl)benzylamine gave the title compound as a colorless oil (66%). 1H NMR (CDCl3, 300 MHz) δ 8.20 (d, J=7.9 Hz, 1H), 7.91 (d, J=7.9 Hz, 1H), 7.76-7.41 (m, 6H), 7.32 (d, J=7.5 Hz, 1H), 6.72 (d, J=7.5 Hz, 1H), 4.19-4.11 (m, 4H), 3.63 (s, 2H), 1.96-1.84 (m, 2H), 1.63-1.47 (m, 2H), 1.45-1.20 (m, 16H), 0.87 (t, J=6.8 Hz, 3H). HPLC (Condition A), Rt: 5.41 min (HPLC purity: 100%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07592477B2
출처 데이터셋uspto-grants-2009_09
ORD IDord-13cd9cde243040d79314288bc01a04e1
출처 메모uspto-grants-2009_09