HCID 67188044, 화합물 → HCID 67188008, 화합물

HRID 735964

반응식

HRID 735964 반응식
[CH2:1]([C:12]1[N:16]=[C:15]([C:17]2[CH:18]=[C:19]([CH:22]=[CH:23][CH:24]=2)[CH:20]=O)[O:14][N:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].Br.[C:26]1([C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)[CH:31]=[CH:30][CH:29]=[C:28]([CH2:32][NH2:33])[CH:27]=1>>[C:26]1([C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)[CH:31]=[CH:30][CH:29]=[C:28]([CH2:32][NH:33][CH2:20][C:19]2[CH:22]=[CH:23][CH:24]=[C:17]([C:15]3[O:14][N:13]=[C:12]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[N:16]=3)[CH:18]=2)[CH:27]=1

참가 물질

3

반응물 2

HCID 67188044HCID 67188044, 화합물HCID 865985383-(3-Undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde

생성물 1

HCID 67188008HCID 67188008, 화합물

실험 절차

The same procedure as employed in the preparation of Example 357 (step a) but using 3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde and 1,1′-biphenyl-3-ylmethylamine hydrobromide gave the title compound as an oil. M+(LC/MS(ESI)): 496.5. HPLC (Condition A), Rt: 4.99 min (HPLC purity: 87.7%).

후처리

  1. customThe same procedure as employed in the preparation of Example 357 (step a) but

출처 및 근거

ORD 기록
ord-522650b048b24b079127066066627ee1
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07592477B2

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