Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one → (3-Nitro-phenyl)-(4-pyridin-3-yl-pyrimidin-2-yl)-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one | HCID 567033 | — |
| 반응물 | 3-Nitrophenylguanidine Nitrate | HCID 178512513 | — |
| 생성물 | (3-Nitro-phenyl)-(4-pyridin-3-yl-pyrimidin-2-yl)-amine | HCID 9860872 | 69.7% |
반응 단계
3-Nitrophenyl-guanidine nitrate (28 g, 0.12 mol) and 3-dimethylamino-1-(3-pyridyl)-2-propen-1-one (16.9 g, 0.09 mol) were reacted according to the same procedure as Step 1.3 of Preparation 1 to give N-(3-nitrophenyl)-4-(3-pyridyl)-2-pyrimidine-amine (18.4 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07595323B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-18ee62cb361345d79978b33f89b667b2 |
| 출처 메모 | uspto-grants-2009_09 |