4-Fluorobenzaldehyde → E-4-fluorostyryl 4-fluorobenzyl sulfone

HRID 736543노트

반응식

HRID 736543 반응식
[F:1][C:2]1[CH:15]=[CH:14][C:5]([CH2:6][S:7]([CH2:10][C:11](O)=O)(=[O:9])=[O:8])=[CH:4][CH:3]=1.[F:16][C:17]1[CH:24]=[CH:23][C:20](C=O)=[CH:19][CH:18]=1>>[F:1][C:2]1[CH:15]=[CH:14][C:5]([CH2:6][S:7](/[CH:10]=[CH:11]/[C:20]2[CH:23]=[CH:24][C:17]([F:16])=[CH:18][CH:19]=2)(=[O:9])=[O:8])=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 680234-FluorobenzaldehydeHCID 11447598[(4-Fluorobenzyl)sulfonyl]acetic acid

생성물 1

HCID 9948064E-4-fluorostyryl 4-fluorobenzyl sulfone수율 73%

실험 절차

A solution of 4-fluorobenzyl sulfonylacetic acid (0.01 mol) and 4-fluorobenzaldehyde (0.01 mol) was subjected to Procedure 1, Part B. The title compound was obtained in 73% yield.

출처 및 근거

ORD 기록
ord-c44cff11e7ab499e8bdf6223ad8ee5ed
출처 데이터셋
uspto-grants-2009_09
특허 번호
US07595347B2

반응 노트

불러오는 중…