Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexamethylcyclotrisiloxane → Nonamethyltetrasiloxanyl 2-methylprop-2-enoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexamethylcyclotrisiloxane | HCID 10914 | — |
| 반응물 | Trifluoromethanesulfonic acid | HCID 62406 | — |
| 반응물 | 2-Propenoic acid, 2-methyl-, trimethylsilyl ester | HCID 2733839 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | Nonamethyltetrasiloxanyl 2-methylprop-2-enoate | HCID 12991985 | — |
반응 단계
5 g of hexamethylcyclotrisiloxane, 3.5 g of trimethylsilyl methacrylate, 0.016 g of trifluoromethane sulfonic acid were stirred for 24 h at room temperature. 0.5 ml of triethylamine was then added, and the salts were filtered to furnish nonamethyl-1-methacryloyloxy-tetrasiloxane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07595370B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-9f5b029e75fd41529db837badcc7691e |
| 출처 메모 | uspto-grants-2009_09 |