Isocyanate → (4-Isocyanatobutyl)cyclohexane

반응식

[N-:1]=[C:2]=[O:3].[CH:4]1([CH2:10][CH2:11][CH2:12][CH2:13]N)[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1>>[N:1]([CH2:13][CH2:12][CH2:11][CH2:10][CH:4]1[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1)=[C:2]=[O:3]

참가 물질

반응물 2

HCID 105034Isocyanate2회

HCID 30589564-Cyclohexylbutan-1-amine

생성물 1

HCID 22590210(4-Isocyanatobutyl)cyclohexane수율 91%

실험 절차

Following the synthetic procedure of 4b′ as described in Example 17, isocyanate 4d′ (91% yield) was synthesized from 4-(cyclohexyl)butylamine as an oil. 1H-NMR (CDCl3) δ0.80-0.95 (m, 2H), 1.10-1.30 (m, 6H), 1.32-1.45 (m, 2H), 1.52-1.75 (m, 7H), 3.28 (t, J=6.6 Hz, 2H).

출처 및 근거

ORD 기록: ord-43fa33f0591140539a4d93ec59359943
출처 데이터셋: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07595403B2

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