Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Chlorodifluoromethoxy)aniline → 6-chloro-N-(4-(chlorodifluoromethoxy)phenyl)-5-iodonicotinamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Chlorodifluoromethoxy)aniline | HCID 572793 | — |
| 반응물 | 6-Chloro-5-iodonicotinic acid | HCID 22271477 | — |
| 생성물 | 6-chloro-N-(4-(chlorodifluoromethoxy)phenyl)-5-iodonicotinamide | HCID 86702626 | — |
반응 단계
The title compound was prepared in an analogous fashion to that described in Stage 11.2 using 6-chloro-5-iodonicotinic acid and 4-(chlorodifluoromethoxy)aniline to afford an off-white powder. HPLC (Condition 4) tR=6.47 min, UPLC-MS (Condition 3) tR=1.26 min, m/z=456.8 [M−H]−.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08829195B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-f324f55a49224e8a8e5a5fed04932a04 |
| 출처 메모 | uspto-grants-2014_09 |