참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | t-Butyl bromide | HCID 10485 | — |
| 반응물 | 6-Nitro-1H-indole | HCID 78502 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 촉매 | Tetrabutylammonium Iodide | HCID 67553 | — |
| 촉매 | Zinc trifluoromethanesulfonate | HCID 104671 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 3-(tert-Butyl)-6-nitro-1h-indole | HCID 57470198 | 22.2% |
반응 단계
To a mixture of 6-nitroindole (1 g, 6.2 mmol), zinc triflate (2.06 g, 5.7 mmol) and TBAI (1.7 g, 5.16 mmol) in anhydrous toluene (11 mL) was added DIEA (1.47 g, 11.4 mmol) at room temperature under nitrogen. The reaction mixture was stirred for 10 min at 120° C., followed by addition of t-butyl bromide (0.707 g, 5.16 mmol). The resulting mixture was stirred for 45 min at 120° C. The solid was filtered off and the filtrate was concentrated to dryness and purified by column chromatography on silica gel (Pet.Ether./EtOAc 20:1) to give 3-tert-butyl-6-nitro-1H-indole as a yellow solid (0.25 g, 19%). 1H NMR (CDCl3) δ 8.32 (d, J=2.1 Hz, 1H), 8.00 (dd, J=2.1, 14.4 Hz, 1H), 7.85 (d, J=8.7 Hz, 1H), 7.25 (s, 1H), 1.46 (s, 9H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08829204B2 |
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| 출처 데이터셋 | uspto-grants-2014_09 |
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| ORD ID | ord-f2ad71930ecb4773ba351e9d93c9dc4e |
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| 출처 메모 | uspto-grants-2014_09 |
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