2-Bromobutane → 3-sec-Butyl-1H-indol-6-ylamine
반응식
[N+:1]([C:4]1[CH:12]=[C:11]2[C:7]([CH:8]=[CH:9][NH:10]2)=[CH:6][CH:5]=1)([O-])=O.Br[CH:14]([CH2:16][CH3:17])[CH3:15]>CC#N>[CH:14]([C:8]1[C:7]2[C:11](=[CH:12][C:4]([NH2:1])=[CH:5][CH:6]=2)[NH:10][CH:9]=1)([CH2:16][CH3:17])[CH3:15]참가 물질
4
실험 절차
3-sec-Butyl-1H-indol-6-ylamine (B-14) was synthesized following the general scheme above starting from 6-nitroindole and 2-bromobutane. Overall yield (20%). HPLC ret. time 2.32 min, 10-99% CH3CN, 5 min run; ESI-MS 189.5 m/z (MH+).
후처리
- customOverall yield (20%)
출처 및 근거
- ORD 기록
- ord-9e49ae8cd83446ca958e78fb7ba17cdc
- 출처 데이터셋
- uspto-grants-2014_09
- 특허 번호
- US08829204B2
반응 노트
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