Iodocyclopentane → 3-Cyclopentyl-1H-indol-6-ylamine
반응식
[N+:1]([C:4]1[CH:12]=[C:11]2[C:7]([CH:8]=[CH:9][NH:10]2)=[CH:6][CH:5]=1)([O-])=O.I[CH:14]1[CH2:18][CH2:17][CH2:16][CH2:15]1>CC#N>[CH:14]1([C:8]2[C:7]3[C:11](=[CH:12][C:4]([NH2:1])=[CH:5][CH:6]=3)[NH:10][CH:9]=2)[CH2:18][CH2:17][CH2:16][CH2:15]1참가 물질
4
실험 절차
3-Cyclopentyl-1H-indol-6-ylamine (B-15) was synthesized following the general scheme above starting from 6-nitroindole and iodo-cyclopentane. Overall yield (16%). HPLC ret. time 2.39 min, 10-99% CH3CN, 5 min run; ESI-MS 201.5 m/z (MH+).
후처리
- customOverall yield (16%)
출처 및 근거
- ORD 기록
- ord-c3c0b43630de4ff99b8c0cc7f36344df
- 출처 데이터셋
- uspto-grants-2014_09
- 특허 번호
- US08829204B2
반응 노트
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