Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromoethyl ethyl ether → 3-(2-Ethoxy-ethyl)-1H-indol-6-ylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromoethyl ethyl ether | HCID 61141 | — |
| 반응물 | 6-Nitro-1H-indole | HCID 78502 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 3-(2-Ethoxy-ethyl)-1H-indol-6-ylamine | HCID 57470202 | — |
반응 단계
3-(2-Ethoxy-ethyl)-1H-indol-6-ylamine (B-16) was synthesized following the general scheme above starting from 6-nitroindole and 1-bromo-2-ethoxy-ethane. Overall yield (15%). HPLC ret. time 1.56 min, 10-99% CH3CN, 5 min run; ESI-MS 205.1 m/z (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08829204B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-855bda40a3204eccaaf5f6d6449f9cea |
| 출처 메모 | uspto-grants-2014_09 |