Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenol → 6-(3-Hydroxypent-3-yl)pyridin-2-methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | Thiophenol | HCID 7969 | — |
| 반응물 | 1-Bromo-3-(3,4-dimethoxybenzyloxy)-5-fluorobenzene | HCID 19426985 | — |
| 반응물 | 2-Bromo-6-(tert-butyldiphenylsiloxy)methylpyridine | HCID 23370237 | — |
| 생성물 | 6-(3-Hydroxypent-3-yl)pyridin-2-methanol | HCID 19426993 | — |
반응 단계
Following the procedure described for Phenol 2, Step 2 and for Phenol 7, Step 3, but substituting 6-bromo(O-tert-butyldiphenylsilyl)pyridin-2-methanol form Step 4 for 1-bromo-3-(3,4-dimethoxybenzyloxy)-5-fluorobenzene, the title compound was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05552437 |
| 출처 데이터셋 | uspto-grants-1996_09 |
| ORD ID | ord-5323fae251334457994cf16671f58341 |
| 출처 메모 | uspto-grants-1996_09 |