Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 4-Imidazolidinone, 3-(diphenylmethyl)-1-methyl-2-thioxo-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Ethyl N-methylaminoacetate hydrochloride | HCID 171173 | — |
| 반응물 | Benzhydryl isothiocyanate | HCID 520742 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 4-Imidazolidinone, 3-(diphenylmethyl)-1-methyl-2-thioxo- | HCID 11150625 | — |
반응 단계
The title compound was prepared by the procedure described in Example 1 using 11.25 g of benzhydryl-isothiocyanate, 7.68 g of sarcosine ethyl ester hydrochloride, 12 g of triethyl amine, and 200 mL of chloroform. The title compound was obtained (7.40 g) as an off-white solid, m.p. 139°-141° C. Anal. Calcd. for C17H16N2O S: C, 68.89; H, 5.44; N, 9.45. Found: C, 68.92; H, 5.43; N, 9.58. Mass spectrum (El, M.+) m/z 296.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05554607 |
| 출처 데이터셋 | uspto-grants-1996_09 |
| ORD ID | ord-bd0b8e661d7844e99bc0f045247d5240 |
| 출처 메모 | uspto-grants-1996_09 |