Thionyl Chloride → HCID 19047521, 화합물

HRID 742492노트

반응식

HRID 742492 반응식
[CH2:1]([O:3][C:4]([C:6]([CH3:12])([CH3:11])[CH2:7][C:8](O)=[O:9])=[O:5])[CH3:2].S(Cl)([Cl:15])=O>>[CH2:1]([O:3][C:4]([C:6]([CH3:12])([CH3:11])[CH2:7][C:8]([Cl:15])=[O:9])=[O:5])[CH3:2]

참가 물질

3

반응물 2

HCID 24386Thionyl ChlorideHCID 1429488732980-28-2

생성물 1

HCID 19047521HCID 19047521, 화합물

실험 절차

A mixture of 3-ethoxycarbonyl-3,3-dimethylpropionic acid (1 g) and 3 ml of thionyl chloride was stirred at room temperature for 20 hours. The excess thionyl chloride was removed in vacuo to afford 1.1 g of 3-ethoxycarbonyl-3,3-dimethylpropionyl chloride.

후처리

  1. customThe excess thionyl chloride was removed in vacuo

출처 및 근거

ORD 기록
ord-6be85a7089ba4a5c95b68c1e86a42a63
출처 데이터셋
uspto-grants-1996_09
특허 번호
US05554620

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