2-(2-(3-Methoxyphenyl)ethyl)phenol → Potassium 2-[2-(3-methoxyphenyl)ethyl]phenolate
반응식
CC(C)([O-])C.[K+:6].[CH3:7][O:8][C:9]1[CH:10]=[C:11]([CH2:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2[OH:23])[CH:12]=[CH:13][CH:14]=1>CC(N(C)C)=O>[CH3:7][O:8][C:9]1[CH:10]=[C:11]([CH2:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2[O-:23])[CH:12]=[CH:13][CH:14]=1.[K+:6]참가 물질
4
실험 절차
9.83 g of potassium t-butoxide were added, whilst ice-cooling and stirring, to a solution of 20.0 g of 2-[2-(3-methoxyphenyl)ethyl]phenol (prepared as described in Preparation 20) in 50 ml of dimethylacetamide, and the resulting mixture was stirred at the same temperature for 30 minutes, to give potassium 2-[2-(3-methoxyphenyl)ethyl]phenolate.
후처리
- temperaturecooling
출처 및 근거
- ORD 기록
- ord-ace70d24f700402b8a7b86845c571d2b
- 출처 데이터셋
- uspto-grants-1996_09
- 특허 번호
- US05556864
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