Ethyl 3-(naphthalen-2-yl)propanoate → 2-Naphthalenepropanol
반응식
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][CH2:12][C:13](OCC)=[O:14].[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][CH2:12][CH2:13][OH:14]참가 물질
4
실험 절차
Following a procedure similar to that described in the first part of Preparation 4, the whole of this ethyl 3-(2-naphthyl)propionate was reacted with 668 mg of lithium aluminum hydride in tetrahydrofuran at room temperature for 1.5 hours. At the end of this time, the reaction mixture was worked up and purified as described in the first part of Preparation 4, to give 3.29 g of 3-(2-naphthyl)propanol as a colorless oil.
후처리
- customthat described in the first part of Preparation 4
- custompurified
- customas described in the first part of Preparation 4
출처 및 근거
- ORD 기록
- ord-369aca6a51a94293a501737d7028e18b
- 출처 데이터셋
- uspto-grants-1996_09
- 특허 번호
- US05556864
반응 노트
불러오는 중…