1-Benzhydryl-3-(cyclopropylamino)azetidine dihydrochloride → 3-(Cyclopropylamino)azetidine dihydrochloride

반응식

[ClH:1].Cl.C(NC1CNC1)C.Cl.Cl.C([N:25]1[CH2:28][CH:27]([NH:29][CH:30]2[CH2:32][CH2:31]2)[CH2:26]1)(C1C=CC=CC=1)C1C=CC=CC=1>>[ClH:1].[ClH:1].[CH:30]1([NH:29][CH:27]2[CH2:28][NH:25][CH2:26]2)[CH2:32][CH2:31]1

참가 물질

반응물 2

HCID 194236711-Benzhydryl-3-(cyclopropylamino)azetidine dihydrochloride

HCID 22121198N-ethylazetidin-3-amine dihydrochloride

생성물 1

HCID 194236593-(Cyclopropylamino)azetidine dihydrochloride

실험 절차

3-(Cyclopropylamino)azetidine dihydrochloride was prepared under the conditions described in Example 9 for 3-(ethylamino)azetidine dihydrochloride, but starting with 5.4 g of 1-benzhydryl-3-(cyclopropylamino)azetidine dihydrochloride. 2.25 g of 3-(cyclopropylamino)azetidine dihydrochloride are obtained in the form of a colorless solid, melting point 140° C.

후처리

custom3-(Cyclopropylamino)azetidine dihydrochloride was prepared under the conditions

출처 및 근거

ORD 기록: ord-0baaa8c154c04ed3957758a64f01c626
출처 데이터셋: uspto-grants-1996_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05556861

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