1,1,2,2,3,3,4,4,5,5,6,6-Dodecafluoroheptan-1-OL → Octafluoro-1-pentanol

HRID 743912노트

반응식

HRID 743912 반응식
FC(F)(C)[C:3](F)(F)[C:4]([F:16])([F:15])[C:5]([F:14])([F:13])[C:6]([F:12])([F:11])[C:7]([F:10])([F:9])[OH:8]>FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F>[F:15][C:4]([F:16])([CH3:3])[C:5]([F:13])([F:14])[C:6]([F:11])([F:12])[C:7]([F:10])([F:9])[OH:8]

참가 물질

3

반응물 1

HCID 222779521,1,2,2,3,3,4,4,5,5,6,6-Dodecafluoroheptan-1-OL

생성물 1

HCID 216319Octafluoro-1-pentanol

시약·촉매·용매 1

HCID 12675Perfluoropentane용매2회

실험 절차

A 1.0 mL portion of dodecafluoroheptanol (PCR) was added to 1.0 mL of dodecafluoropentane to form a clear, homogenous solution. The same quantity of octafluoropentanol in dodecafluoropentane yielded two clear, non-mixing phases. The addition of 2.0 to 4.0 mL water to the dodecafluoroheptanoldodecafluoropentane yielded two non-mixing phases. Upon cooling to 4° C. the two clear phases changed to three clear phases.

후처리

  1. customto form a clear, homogenous solution

출처 및 근거

ORD 기록
ord-c2332f26e8b04f5fab3d582f6daffe4d
출처 데이터셋
uspto-grants-1996_09
특허 번호
US05558855

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