1-Iodopropane → 2-Propenoic acid, 3-(3-methoxy-4-propoxyphenyl)-, ethyl ester

HRID 744106

반응식

HRID 744106 반응식
[OH:1][C:2]1[CH:14]=[CH:13][C:5](/[CH:6]=[CH:7]/[C:8]([O:10][CH2:11][CH3:12])=[O:9])=[CH:4][C:3]=1[O:15][CH3:16].[CH2:17](I)[CH2:18][CH3:19]>>[CH3:16][O:15][C:3]1[CH:4]=[C:5]([CH:13]=[CH:14][C:2]=1[O:1][CH2:17][CH2:18][CH3:19])/[CH:6]=[CH:7]/[C:8]([O:10][CH2:11][CH3:12])=[O:9]

참가 물질

3

반응물 2

HCID 336431-IodopropaneHCID 736681Ethyl Ferulate

생성물 1

HCID 64507182-Propenoic acid, 3-(3-methoxy-4-propoxyphenyl)-, ethyl ester수율 91.4%

실험 절차

Following a procedure similar to that described in Preparation 116, but using 11.11 g of ethyl (E)-4-hydroxy-3-methoxycinnamate and 10.20 g of propyl iodide, 12.08 g of the title compound were obtained.

후처리

  1. customthat described in Preparation 116

출처 및 근거

ORD 기록
ord-9cdaba3b1f3f45a387ebe9358e40848f
출처 데이터셋
uspto-grants-1996_09
특허 번호
US05559109

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