Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylresorcinol → 3-(Cyclohexylmethoxy)-2-methylphenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylresorcinol | HCID 11843 | — |
| 반응물 | Cyclohexane, (bromomethyl)- | HCID 137636 | — |
| 생성물 | 3-(Cyclohexylmethoxy)-2-methylphenol | HCID 43143282 | — |
반응 단계
Alkylation of 2-methylbenzene-1,3-diol using (bromomethyl)cyclohexane following the method used in Example 154 gave 3-(cyclohexylmethoxy)-2-methylphenol. Yield (0.58 g, 37%): 1H NMR (400 MHz, CDCl3) δ 6.98 (t, J=8.0 Hz, 1H), 6.42 (t, J=7.6 Hz, 2H), 4.60 (bs, 1H), 3.72 (d, J=6.4 Hz, 2H), 2.12 (s, 3H), 1.68-1.89 (m, 6H), 1.16-1.35 (m, 3H), 1.01-1.11 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08829244B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-91ea1935be7d4b88b8f46a9d71815531 |
| 출처 메모 | uspto-grants-2014_09 |