Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoate → Benzoate maleate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoate | HCID 242 | — |
| 반응물 | Maleic Acid | HCID 444266 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Benzoate maleate | HCID 68560292 | — |
반응 단계
In 3 mL of ethyl acetate was dissolved 0.25 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate, and 0.07 g of maleic acid was added thereto, after which the resulting mixture was heated to effect dissolution. The reaction mixture was cooled and the crystals precipitated were collected by filtration to obtain 0.15 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate maleate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07087594B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-595bfc092f2a49439306456243cac199 |
| 출처 메모 | uspto-grants-2006_08 |