Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalic Acid → Carbonate oxalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalic Acid | HCID 971 | — |
| 반응물 | Carbonate Ion | HCID 19660 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Carbonate oxalate | HCID 88099579 | — |
반응 단계
In 7 mL of ethyl acetate was dissolved 0.31 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate, and to the solution was added a solution of 0.10 g of oxalic acid in 1 mL of ethyl acetate, after which the resulting mixture was stirred at room temperature. The crystals precipitated were collected by filtration to obtain 0.34 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate oxalate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07087594B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-969acd0d0f2e422ba1015f8da344886c |
| 출처 메모 | uspto-grants-2006_08 |