Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylformamide → 6-Diethylamino-3,8-di-(pyrrolidinomethyleneamino)-phenanthridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylformamide | HCID 12051 | — |
| 반응물 | 1-Pyrrolidinecarboxaldehyde | HCID 77372 | — |
| 반응물 | 3,8-Diamino-6-diethylaminophenanthridine | HCID 23314007 | — |
| 생성물 | 6-Diethylamino-3,8-di-(pyrrolidinomethyleneamino)-phenanthridine | HCID 13345880 | 66% |
반응 단계
As in Example 14, but using 3,8-diamino-6-diethylaminophenanthridine and N-formylpyrrolidine instead of 3,8-diamino-6-dimethylaminophenanthridine and N,N-diethylformamide. Yield 66%, melting point 149°-150° C. (chloroform/petroleum ether (60°-80° C.)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04599409 |
| 출처 데이터셋 | uspto-grants-1986_07 |
| ORD ID | ord-97ac297e36e14eefa5a32fef4f37b4e5 |
| 출처 메모 | uspto-grants-1986_07 |