Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,10-Decanediamine → N-(10-aminodecyl)-aminomethanephosphonic acid monohydrate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,10-Decanediamine | HCID 1317 | — |
| 반응물 | P-(Chloromethyl)phosphonic acid | HCID 75723 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-(10-aminodecyl)-aminomethanephosphonic acid monohydrate | HCID 86740900 | — |
반응 단계
Chloromethanephosphonic acid (5.5 g, 42 mmoles) and 1.10-diaminodecane (44 g, 255 mmoles) were heated under reflux in water (200 cm3) for 20 hours. The water was removed and ethanol (400 cm3) added to the solid residue. The phosphonic acid was filtered off and dried. The crude yield was 11.4 g (87%). A sample was purified by recrystallization from water/ethanol to give N-(10-aminodecyl)-aminomethanephosphonic acid monohydrate as a fine white crystalline solid having a melting point of 238° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04600429 |
| 출처 데이터셋 | uspto-grants-1986_07 |
| ORD ID | ord-09381e4a41b946cbb8ee07e8ed0fa10d |
| 출처 메모 | uspto-grants-1986_07 |